SinoTechIntel Academic Portal
🏛️ Indexed Academic Journal

Journal of Central South University

Access authentic peer-reviewed engineering methodologies, experimental datasets, and scientific literature published in this journal on SinoTechIntel.

Total Research Papers: 152
Access: 100% Free Open Access
Browse by Publication Year & VolumeReset All Filters ✕

Published Research PapersFiltered: Year 2025 • 32

Showing 25 of 152 peer-reviewed papers with full Graphical Abstracts.

Original ResearchVol. 32, Issue 11 • pp. 4196-4209DOI: 10.1007/s11771-025-6123-zJan 15, 2025

Experimental study and creep constitutive modeling for 2219 aluminum alloy under tension and compression conditions

Authors: LI Shuang-bo, MAO Xiao-bo, ZHAN Li-hua, YANG You-liang, LIU Chun-hui, ZENG Quan-qing

The creep deformation and mechanical properties of 2219 aluminum alloy were experimentally investigated under both tension and compression at the temperature of 165 ℃ for different time. The results indicated that the creep deformation under tensile stress was greater than that under compressive stress. As the stress level increases, the compressive creep rate showed more significant increase. The yield strength after compressive stress creep-ageing was higher than that after stress-free ageing, with the lowest strength observed in the tensile-aged sample. Overall, the average phase length after compressive stress creep-ageing was larger than after tensile stress ageing. Under tensile stress, the number and size of precipitates at small angles to the stress direction were larger than those perpendicular to the stress direction. In contrast, under compressive stress, this relationship was reversed, and the preferential orientation of phases became more pronounced with ageing time. A unified, physics-based creep-ageing constitutive model, accounting for the orientation of precipitation, was developed for both tensile and compressive stress conditions. The predicted results were in good agreement with the experimental data. These findings, along with the developed model, provide a theoretical and simulation basis for precise creep-ageing forming of components under complex stresses.

Experimental study and creep constitutive modeling for 2219 aluminum alloy under tension and compression conditions
Graphical Abstract
Original ResearchVol. 32, Issue 11 • pp. 4228-4247DOI: 10.1007/s11771-025-6126-9Jan 15, 2025

Prediction of macroscopic abnormally coarse grain during solid solution of Ti-10V-2Fe-3Al alloy based on dynamic recrystallization kinetics

Authors: ZHANG Yu-sen, CHEN Lei, GAO Xiao-peng, GUO Cong-de, CAI Xing-zhou, JIN Miao, MA Xiao-cong

After the hot deformation sample of Ti-10V-2Fe-3Al alloy was treated by solid solution in the α+β two-phase region, the coarse β grains that often appeared in the β single phase region were observed in the local region, indicating that the abnormal grain growth occurred in the local microstructural region, and the macrostructure also showed abnormally coarse grains (ACGs). The dynamic recrystallization (DRX) behavior of Ti-10V-2Fe-3Al titanium alloy was systematically investigated through hot compression tests on the Gleeble-3800 system. The DRX model of β grains was established, and the quantitative correlation between DRX characteristics and the appearance of ACG was clarified. Based on these results, a numerical simulation platform was developed to realize the visual prediction of ACG distribution. The results show that the increase of deformation temperature and the decrease of strain rate both contribute to a significant increase in the grain size (dDRX) and volume fraction (XDRX) of DRXed grains. However, the proper XDRX and smaller dDRX at low deformation temperature and high strain rate make the macro and microstructure show ACGs after solid solution. Interestingly, if the DRX degree is excessive or insufficient, ACGs cannot be produced, indicating that ACGs are solid solution products based on the appropriate DRX degree. According to the flow curves and statistical results of microstructure, the quantitative model of DRX kinetics and DRX grain size model were constructed, and the quantitative criterion model that is related to the formation of ACG with grain size (dDRX) and volume fraction (XDRX) of DRXed grains as the key parameters was established, i. e., dDRX£2.60 μm, 72.5%£XDRX£87.9%. By integrating the subroutine of coarse grain criterion, the isothermal compression process of cylindrical samples and the actual die forging process of H-shaped parts were simulated by DEFORM-3D software of finite element (FE), respectively, and the visual prediction of the distribution of macroscopic ACGs was realized. There is a good consistency between the tested results and the simulated results, indicating a strong correlation between macroscopic ACGs and microscopic DRX.

Prediction of macroscopic abnormally coarse grain during solid solution of Ti-10V-2Fe-3Al alloy based on dynamic recrystallization kinetics
Graphical Abstract
Original ResearchVol. 32, Issue 9 • pp. 3657-3674DOI: 10.1007/s11771-025-6065-5Jan 15, 2025

Deformation characteristics and interfacial damage of CRTS II slab track joints under operating temperature conditions

Authors: DONG Bo, CHEN Zhi-yuan, ZHU Hao, CAI Xiao-pei, ZHANG Xing, HE Xu

Arching and cracking of joints between slabs have become a problem in China Railway Track System (CRTS) II slab track. The slab track is susceptible to complex temperature variations as a longitudinal continuous structure. Based on measured data, a thermal-mechanical coupling model of the track was established. The deformation characteristics and interfacial damage behavior of joints under typical temperature fields were studied. The findings indicate that the annual extreme temperature range of the slab track, fluctuates from −1.4 to 49.8 ℃. The annual temperature gradient within the vertical depth range of 0 to 0.2 m of the track varies between −16.19 ℃/m and 30.15 ℃/m. The vertical deformation of joints is significantly influenced by high temperatures, with a maximum measured deformation of 0.828 mm. The joint seams are primarily affected by low temperatures, which lead to a separation of 0.9 to 1.0 mm. Conversely, interlayer damage of joints is predominantly influenced by elevated temperatures. In summer, the maximum ratio of interface damage area in the joint can reach up to 95%, with the maximum debonding area ratio can be as high as 84%. The research results can provide help for joint damage regularity and deformation control of CRTS II slab track.

Deformation characteristics and interfacial damage of CRTS II slab track joints under operating temperature conditions
Graphical Abstract
Original ResearchVol. 32, Issue 12 • pp. 4955-4967DOI: 10.1007/s11771-025-6142-9Jan 15, 2025

Effects of shaft and tunnel portal on coupled aerodynamic characteristics of 600 km/h superconducting maglev train

Authors: PAN Shen-gong, ZHANG Lei, WANG Tian-tian, YU Qing-song, LIN Tong-tong, XU Shu

To address the severe aerodynamic effects caused by a 600 km/h superconducting maglev train passing through a tunnel at full speed, this study systematically investigates the coupled influence of auxiliary facility parameters including the shaft (location L, cross sectional dimension W, height h), tunnel portal (cross sectional area S), and openings (spacing D, side length F) on the evolution of tunnel aerodynamic effects. By integrating three dimensional unsteady flow field numerical simulations with a dynamic model testing system, the research notably reveals the regulatory mechanisms of these parameters on the evolution characteristics of the initial compression wave pressure gradient and the multi peak structure of micro-pressure waves. The results show that shaft parameters significantly affect the initial compression wave. Both the wave amplitude and gradient exhibit a linear negative correlation with cross sectional dimension W and a linear positive correlation with location L, while demonstrating a nonlinear relationship with height h, the amplitude follows a cubic polynomial trend, and the gradient initially increases before plateauing. Under the configuration W=8 m, L=50 m, and h=20 m, substantial reductions in both compression wave amplitude and gradient were achieved. The portal cross sectional area S shows a "U-shaped" relationship with the compression wave gradient, with the maximum gradient reduction of 53.24% occurring at S=210 m2, a result comparable to that achieved with optimized opening parameters (D=15 m, F=3.5 m, 53.96%). Regarding micro-pressure waves, the amplitude measured 20 m from the tunnel exit shows a linear positive correlation with shaft parameters L and W, while the influence of h saturates beyond 50 m. Reductions exceeding 54% were achieved with portal parameters, either at S=210 m2 or using the optimized opening configuration. Furthermore, micro-pressure waves near the portal exhibit a consistent dual peak structure: the first peak originates from the train entry compression wave, and the second results from further wave compression after tunnel exit. The opening location governs selective peak regulation openings near the portal entrance primarily suppress the first peak with minimal impact on the second, whereas centrally located openings reduce the first peak but can amplify the second by up to 3%. Based on these insights, an optimized parameter configuration is proposed: a shaft with a cross-sectional dimension ≥8 m located 50 m from the portal, a portal cross sectional area of 210 m2, and openings spaced at 15 m intervals. This configuration can reduce the initial compression wave gradient by over 50%. The results provide a theoretical foundation for controlling aerodynamic effects of superconducting maglev train.

Effects of shaft and tunnel portal on coupled aerodynamic characteristics of 600 km/h superconducting maglev train
Graphical Abstract
Original ResearchVol. 32, Issue 12 • pp. 5105-5123DOI: 10.1007/s11771-025-6152-7Jan 15, 2025

Full-scale test of the effects of crosswinds on the operating posture of passenger trains

Authors: PANG Jia-hong, ZHOU Wei, SHI Chong, LI Tian, LIU Dong-run

Considering passenger trains' key role in remote regions, this study employed machine vision technology to monitor five posture parameters of the second car of a conventional passenger train, aiming to investigate the influence of windbreaks and crosswinds along railways on the operating postures of conventional passenger trains. The study found that when passing through the anti-wind tunnel with holes, the amplitudes of posture parameters were smaller than those of other windbreaks, demonstrating the superior performance of this windbreak in maintaining posture stability compared to others. In tunnel sections, larger amplitudes of these parameters were observed for the tail car than the head car, while the opposite occurred in non-tunnel sections. Notably, during tunnel transit, their amplitudes did not increase monotonically with speed but peaked at a specific speed that most adversely affected the operating posture. These conclusions have a great significance for improving operating safety under crosswinds.

Full-scale test of the effects of crosswinds on the operating posture of passenger trains
Graphical Abstract
Original ResearchVol. 32, Issue 12 • pp. 4940-4954DOI: 10.1007/s11771-025-6064-6Jan 15, 2025

Effects of middle air shaft and bypass duct on aerodynamic pressure of platform screen doors in high-speed subway stations

Authors: ZHANG Xu, ZHOU Yuan-long, BI Hai-quan, WANG Hong-lin, YU Nan-yang

The aerodynamic pressure disturbances induced by middle air shafts and bypass ducts in subway tunnels pose significant challenges to enhancing train operational speeds. A comprehensive series of full-scale experiments are employed to examine the impact of these structural elements on the aerodynamic pressure characteristics of platform screen doors (PSDs) in high-speed subway stations. The experimental results reveal that peak pressures manifest on PSDs surfaces during two distinct scenarios in high-speed subway systems equipped with middle air shafts. One is compression pressure waves propagated from trains traversing the air shaft, and the other is train nearby flow when trains pass the PSDs directly. The peak positive pressures caused by train passing PSDs are much greater than compression pressure waves. Closing middle air shaft can reduce the passing pressure waves. The installation of bypass ducts at overtaking station entrances effectively mitigates peak negative pressures during train-PSD interactions, achieving a maximum reduction efficiency of 8%. These findings provide valuable insights for optimizing the structural design of high-speed subway tunnel systems.

Effects of middle air shaft and bypass duct on aerodynamic pressure of platform screen doors in high-speed subway stations
Graphical Abstract
Original ResearchVol. 32, Issue 11 • pp. 4613-4632DOI: 10.1007/s11771-025-6124-yJan 15, 2025

Influence of deterioration of CRTSⅢ slab ballastless track irregularity on the safety and stability of high-speed vehicles

Authors: GAO Rui-kai, XIN Tao, GAO Liang, MA Shuai, LIU Xiu-bo

Abstract: As one of the major high-speed railway ballastless track structures in China, CRTSⅢ slab ballastless track has been laid for more than 6500 km. However, there are no detailed studies on its track irregularity deterioration throughout extended service periods, which may threaten the safety and stability of high-speed vehicles (HSV). In this study, a long-term tracking detection of CRTSⅢ slab ballastless track irregularities has been conducted, revealing its annual evolution law. An HSV-track coupled dynamics model was established to investigate the HSV dynamic responses under annual evolution of track irregularities. Considering the potential deterioration of track irregularities to extremely bad condition, the recommended classified limits for irregularity are proposed by analyzing the limit-exceeding probability of the safety and stability indexes of HSV. The results show that: taking 10 m wavelength as a demarcation, longer-wavelength irregularities exhibit larger amplitudes, faster evolution rates and a linear increasing trend, primarily affecting the stability of HSV. Conversely, shorter-wavelength irregularities exhibit smaller amplitudes and an insignificant evolution trend, predominantly affecting the safety of HSV. Furthermore, the periodic irregularity induced by the arching of 32 m simply-supported beam bridge should be paid closer attention to, as their evolution rate significantly surpasses that of irregularities at other wavelengths.

Influence of deterioration of CRTSⅢ slab ballastless track irregularity on the safety and stability of high-speed vehicles
Graphical Abstract
Original ResearchVol. 32, Issue 12 • pp. 4702-4719DOI: 10.1007/s11771-025-6137-6Jan 15, 2025

Aerodynamic characteristics on a full-scale high-speed train bogie with rotating wheelsets

Authors: ZHENG Ze-yuan, WANG Tian-tian, WANG Yu, SHI Fang-cheng, FENG Yong-hua, LIU Hong-kang, ZHAO Chang-long, JIANG Chen

Aerodynamic drag is the dominant factor contributing to energy consumption as the operational speed of high-speed trains increases, necessitating effective aerodynamic optimization strategies. This study investigates the aerodynamic characteristics of the bogie region under two bogie fairing configurations: baseline bogie fairing (BBF) and full bogie fairing (FBF). Both stationary and rotating wheelset conditions are considered. Wind tunnel experiments were conducted on a full-scale bogie model equipped with a wheelset drive system to simulate wheelset rotation. Additionally, numerical simulations were employed to analyze flow structures. Results indicate that the FBF configuration promotes a more uniform front-to-rear pressure distribution in the bogie region. The rotation of the wheelset notably affects the airflow near the wheels and extends its influence throughout the entire bogie region. Specifically, wheelset rotation reduces drag by 6.38% in the BBF configuration but increases drag by 3.5% in the FBF configuration. Further analysis reveals that, in the FBF configuration, aerodynamic drag primarily originates from the wheelsets. The rotating wheelset increases the aerodynamic drag by 18.8% for the rear wheelset, which is attributed to the shift in the pressure curve on the wheelset in the rotating direction. Therefore, the impact of wheelset rotation on aerodynamic characteristics should not be overlooked.

Aerodynamic characteristics on a full-scale high-speed train bogie with rotating wheelsets
Graphical Abstract
Original ResearchVol. 32, Issue 11 • pp. 4574-4592DOI: 10.1007/s11771-025-6130-0Jan 15, 2025

Dynamic response characteristics and failure mechanisms of a high-steep bedding rock slope under successive earthquakes in a high-seismic-intensity zone via discrete element method and shaking table tests

Authors: SONG Dan-qing, SHI Wan-peng, HUANG Kun-peng, XIN Chun-lei, LIU Xiao-li, TIAN Yu-xin, ZHANG Bing-hui

Steep bedding slopes are widely distributed in Southwestern China’s mountainous regions and have complex seismic responses and instability risks, causing casualties and property losses. Considering the high-seismic-intensity environment, the dynamic failure evolution and instability mechanism of high-steep bedding slopes are simulated via the discrete element method and shaking table test. The dynamic response characteristics and cumulative failure effects of slopes subjected to continuous ground motion are investigated. The results show that the dynamic response characteristics of slopes under continuous earthquakes are influenced by geological and topographic conditions. Elevation has a distinct impact on both the slope interior and surface, with amplification effects more pronounced on the surface. The weak interlayers have different influences on the dynamic amplification effect of slopes. Weak interlayers have dynamic magnification effects on the slope surface at relative elevations of 0 −0.33 and 0.82 −1.0 but have weakening effects between 0.33 and 0.82. Moreover, the weak interlayers also have controlling effects on the dynamic instability mode of slopes. The characteristics of intergranular contact failure, fracture propagation, and displacement distribution are analyzed to reveal the dynamic failure evolution and instability mechanism through the discrete-element model. The dynamic instability process of slopes includes three stages: fracture initiation (0−0.2g), fracture expansion (0.2g−0.3g), and sliding instability (0.3g−0.6g). This work can provide a valuable reference for the seismic stability and reinforcement of complex slopes.

Dynamic response characteristics and failure mechanisms of a high-steep bedding rock slope under successive earthquakes in a high-seismic-intensity zone via discrete element method and shaking table tests
Graphical Abstract
Original ResearchVol. 32, Issue 11 • pp. 4593-4612DOI: 10.1007/s11771-025-6129-6Jan 15, 2025

A lithium-ion battery state-of-health prediction model based on physical information constraints and multimodal feature fusion

Authors: XU Hai-ming, YU Tian-jian, FENG En-lai, ZENG Xiao-yan, HU Yu-song, CHEN Lan

Accurate estimation of lithium battery state-of-health (SOH) is essential for ensuring safe operation and efficient utilization. To address the challenges of complex degradation factors and unreliable feature extraction, we develop a novel SOH prediction model integrating physical information constraints and multimodal feature fusion. Our approach employs a multi-channel encoder to process heterogeneous data modalities, including health indicators, raw charge/discharge sequences, and incremental capacity data, and uses multi-channel encoders to achieve structured input. A physics-informed loss function, derived from an empirical capacity decay equation, is incorporated to enforce interpretability, while a cross-layer attention mechanism dynamically weights features to handle missing modalities and random noise. Experimental validation on multiple battery types demonstrates that our model reduces mean absolute error (MAE) by at least 51.09% compared to unimodal baselines, maintains robustness under adverse conditions such as partial data loss, and achieves an average MAE of 0.0201 in real-world battery pack applications. This model significantly enhances the accuracy and universality of prediction, enabling accurate prediction of battery SOH under actual engineering conditions.

A lithium-ion battery state-of-health prediction model based on physical information constraints and multimodal feature fusion
Graphical Abstract
Original ResearchVol. 32, Issue 11 • pp. 4340-4360DOI: 10.1007/s11771-025-6119-8Jan 15, 2025

Stability analysis of inclined bauxite pillar under goaf of coal seam considering principal stress rotation

Authors: LIU Wang, YANG Yu-gui, CHEN Yong, HUANG Bing-xiang, CAI Cheng-zheng, SHANG Run-peng, QIU Chao

The “upper coal and lower bauxite” resource distribution pattern is widespread in China, where mining of the overlying coal seam significantly alters the stress environment of the underlying bauxite layer. This study investigates the stability of inclined bauxite pillars under the influence of stress redistribution caused by coal seam extraction. A theoretical model is developed to calculate the direction and magnitude of principal stresses in the inclined floor strata, and a pillar stability analysis model is established that considers the effect of principal stress rotation. The research employs a combination of theoretical analysis, physical modeling, numerical simulation, and field observation. Findings indicate that stress rotation is most pronounced at both ends of the coal seam goaf, with the maximum clockwise and counterclockwise rotation angles of 19° and −40°, respectively, observed in the bauxite layer. Inclined bauxite pillars are subjected to combined compressive and shear loading. Under such conditions, clockwise rotation of principal stress increases the shear-to-normal stress ratio, thereby reducing pillar stability. Pillars located beneath the coal wall are the first to fail due to stress concentration and principal stress rotation, which can trigger a cascade of instability among the adjacent pillars. The findings provide a theoretical basis and practical guidance for ensuring the safe co-mining of coal seams and bauxite resources.

Stability analysis of inclined bauxite pillar under goaf of coal seam considering principal stress rotation
Graphical Abstract
Original ResearchVol. 32, Issue 11 • pp. 4312-4325DOI: 10.1007/s11771-025-6106-0Jan 15, 2025

Transformation pathways and zinc binding mechanisms in magnetite crystallization: Implications for zinc hydrometallurgy

Authors: LI Chun-xue, WU Jia-hui, ZHANG Wen-chao, SHI Mei-qing, WANG Yun-yan, DUAN Ying, YAN Xu, WANG Qing-wei, MIN Xiao-bo, CHAI Li-yuan

Iron removal from zinc leachate in hydrometallurgy produces large volumes of low-grade, impurity-laden iron waste, posing significant environmental challenges. Magnetite precipitation offers a novel method for iron removal and resource recycling in zinc hydrometallurgy. However, the chemical similarity between ferrous and zinc ions, along with high zinc concentrations, causes zinc co-precipitation, challenging its application. To address this issue, this study utilized electron microscopy to observe key intermediate products in magnetite crystallization and employed EXAFS (extended X-ray absorption fine structure) to analyze their evolutionary mechanisms and zinc-binding configurations. The results indicate that the intermediate products during magnetite formation are sequentially green rust, feroxyhyte (δ-FeOOH), and weakly crystalline nanoparticles, and further analysis revealed that their transformation follows the dissolution-recrystallization mechanism. Furthermore, it was found that intermediate products such as green rust exhibit strong binding with zinc (via adsorption and lattice substitution), which was confirmed as a significant reason for the difficulty in separating zinc from magnetite. This study elucidates the transformation process of intermediate products during magnetite formation and, for the first time, reveals the binding configurations of zinc with these key intermediate products. This has significant implications for the development and optimization of new technologies for the efficient separation of iron and zinc during the magnetite precipitation process.

Transformation pathways and zinc binding mechanisms in magnetite crystallization: Implications for zinc hydrometallurgy
Graphical Abstract
Original ResearchVol. 32, Issue 11 • pp. 4281-4295DOI: 10.1007/s11771-025-6104-2Jan 15, 2025

Interaction and mechanism of sub-micron La2Zr2O7 ceramic with calcium-ferrum-alumina-silicate (CFAS) melt at 1673 K

Authors: CHEN Peng-ju, HE Ling, PAN Ling, TIAN Tian, ZHANG Hao, XIAO Peng, LI Yang

Herein, a sub-micron lanthanum zirconate ceramic (La2Zr2O7, LZO) with a pyrochlore structure was prepared by the sol-gel and high temperature sintering methods. The corrosion behavior and mechanism of calcium-ferrum-alumina-silicate (CFAS) powder (33CaO: 10FeO1.5: 13AlO1.5: 44SiO2) on the sub-micron LZO ceramic at 1673 K was investigated. The results indicate that the average grain size of sub-micron LZO ceramic was 895 nm. The CFAS melt rapidly diffused into the interior of the LZO ceramic wafer and reacted with it to generate high melting point rod-shaped Ca2La8(SiO4)6O2 apatite and m-ZrO2 phases, which can effectively hinder further diffusion of CFAS melt, resulting in a slow increase in corrosion depth with corrosion time. After 30 h of CFAS corrosion at 1673 K, the corrosion depth of the LZO ceramic wafer was only 160.3 μm, demonstrating its excellent high-temperature resistance to CFAS corrosion.

Interaction and mechanism of sub-micron La2Zr2O7 ceramic with calcium-ferrum-alumina-silicate (CFAS) melt at 1673 K
Graphical Abstract
Original ResearchVol. 32, Issue 10 • pp. 4012-4034DOI: 10.1007/s11771-025-6085-1Jan 15, 2025

Mechanical response and failure mechanism of inclined rough jointed rock under true triaxial compression loading

Authors: LIU Han-xiang, JING Hong-wen, YUAN Yong, YIN Qian, WEN Fan, LI Bo

Rock-like specimens containing a joint with different inclination angles and roughness were prepared using 3D printing technology. Then, true triaxial compression loading experiments were conducted on those jointed specimens. The increase in roughness leads to an increase in the axial strength and peak strain. With the increasing inclination angle, the axial strength initially decreases from 30° to 60° and then increases from 60° to 90°. While the peak strain first rises from 30° to 45° and then declines from 45° to 90°. The variation in failure mode results from differences in lateral stress on the joints under different strike directions. Specimens with joint strike parallel to the intermediate principal stress predominantly showed matrix or matrix-joint mixed shear failure, whereas those parallel to the minimum principal stress exhibited matrix shear failure. The analysis results of acoustic emission signals indicate the crack number and shear crack percentage increase with the increasing roughness and first decrease (30° to 60°), then increase (60° to 90°) with the increasing inclination angle. The research results can provide some guidance for the design and support of underground engineering with jointed surrounding rock.

Mechanical response and failure mechanism of inclined rough jointed rock under true triaxial compression loading
Graphical Abstract
Original ResearchVol. 32, Issue 11 • pp. 4159-4179DOI: 10.1007/s11771-025-6084-2Jan 15, 2025

Microstructure evolution and mechanical properties of 2195 Al-Li alloy with different heat-treatment states via friction stir additive manufacturing

Authors: GAO Yong-hui, JIANG Tao, DAI Guo-qing, LI Jun, GUO Yan-hua, SUN Zhong-gang, LIU Chun-hui, ZHAN Li-hua

Friction stir additive manufacturing (FSAM) is an innovative additive manufacturing (AM) method. The various heat treatment conditions of aluminum-lithium alloys using this method have not been widely discussed. In this study, the microstructure evolution and mechanical properties of FSAM 2195 aluminum-lithium alloy in different heat treatment conditions (T3 and T8) were investigated. The results demonstrated that the heat treatment state of 2195 Al-Li alloys was minimally influenced by FSAM as the FSAM temperature exceeded the solid solution temperature. After conducting a single-pass FSAM experiment, a notable grain refinement was observed in the nugget zone (NZ) region compared to the base material (BM). The average grain size of the 2195-T3 alloy decreased from 6.1 to 2.9 μm, while the proportion of high-angle grain boundaries increased from 16.5% to 43.9%. Similarly, the average grain size of the 2195-T8 alloy decreased from 8.9 to 2.8 μm, with an increase in high-angle grain boundary from 37.6% to 59.2%. The tensile strength of the 2195-T3 Al-Li alloy reached 466 and 478 MPa in the NZ of single-pass and lap experiments, respectively. In comparison, the tensile strength of the 2195-T8 Al-Li alloy in the NZ could reach 452 and 481 MPa in single-pass and lap experiments, respectively. These results demonstrate the significant improvements in microstructure and mechanical properties were achieved through the FSAM process.

Microstructure evolution and mechanical properties of 2195 Al-Li alloy with different heat-treatment states via friction stir additive manufacturing
Graphical Abstract
Original ResearchVol. 32, Issue 10 • pp. 3876-3894DOI: 10.1007/s11771-025-6093-1Jan 15, 2025

FeVO4 nanorods decorated natural sepiolite as highly efficient peroxymonosulfate catalyst for tetracycline degradation

Authors: WANG Yu-bo, HU Xiao-long, LI Rui, ZHANG Long, SONG Jun-ying, WANG Li, GUO Qing-bin, GAO Deng-zheng, HUANG Peng, LU Qing, ZHANG Wen-bing

Developing a low-cost stable and high-performance peroxymonosulfate (PMS) catalyst to degrade refractory organic pollutants is still an urgent problem. Herein, this study reported FeVO4 nanorods decorated sepiolite (FeVO4/sepiolite) through simple hydrothermal method as an adsorptive-catalyst for PMS activation to degrade tetracycline (TC). Benefiting from the introduction of sepiolite support, FeVO4 nanorods could be uniformly immobilized onto fibrous sepiolite surface. As a result, FeVO4/sepiolite composite was endowed with excellent adsorption properties, rich surface hydroxyl groups, more reaction active sites, and the stable redox cycle of Fe3+/Fe2+ and V5+/V4+. Therefore, higher TC degradation efficiency (91.19% within 40 min) and larger reaction rate constant (0.1649 min−1) were obtained in FeVO4/sepiolite/PMS system than in FeVO4/PMS system. Besides, the composite presented good stability and reusability, and the effects of application parameters on TC degradation were investigated in detail. Through quenching experiment and electron paramagnetic resonance (EPR) test, it was found that both radical and non-radical species participates in TC degradation, and 1O2 were the main active species. The PMS activation mechanism was proposed, and the possible degradation pathway was also analyzed according to the high performance liquid chromatography-mass spectrometry (HPLC-MS) results. Overall, this work provides meaningful insights for designing natural mineral based PMS activators to effectively remediate antibiotic wastewater.

FeVO4 nanorods decorated natural sepiolite as highly efficient peroxymonosulfate catalyst for tetracycline degradation
Graphical Abstract
Original ResearchVol. 32, Issue 10 • pp. 3834-3844DOI: 10.1007/s11771-025-6073-5Jan 15, 2025

Ablation enhancing on heterogeneous aluminum/titanium alloy films under femtosecond laser burst irradiation

Authors: FU Shun-wei, YIN Kai, LI Xun, YANG Peng-yu, HE Yu-chun, YU Hao-nan, HUANG Yin, ARNUSCH Christopher J.

The femtosecond laser is commonly used for high-quality micromachining of materials. However, the interaction time between the femtosecond laser and the substrate material is extremely short, making it difficult for quantitative measurements and analysis through experiments. In this work, we use a two-temperature model for simulation to study the ablation process of aluminum alloy and aluminum/titanium alloy under femtosecond laser pulse mode. The temperature changes and ablation process of both alloys under femtosecond laser burst irradiation were studied. The study found that when the separation time of sub-pulses was 1 ps, the surface temperature and ablation depth rised with the increase of sub-pulse numbers. A comparison was made between these two alloy types, and enhanced ablation was observed with the heterogeneous aluminum/titanium alloy, up to 34.7% deeper compared to aluminum alloy. Moreover, the detailed theoretical explanation was also discussed. This work provided a basis for efficient ablation of materials with low laser fluence.

Ablation enhancing on heterogeneous aluminum/titanium alloy films under femtosecond laser burst irradiation
Graphical Abstract
Original ResearchVol. 32, Issue 10 • pp. 3781-3792DOI: 10.1007/s11771-025-6087-zJan 15, 2025

Appropriate FeF2 enhancing interface stability of lithium battery with solid-liquid hybrid electrolyte

Authors: TONG Yi-ting, LI Zhuo-jie, PEI Quan, ZHANG Qing-feng, XIE Shu-hong, CHEN Jing

Solid-state electrolytes (SSEs) have attracted much attention due to their high safety and cycling stability for lithium-ion batteries. However, the high interface impedance between the electrode and the solid-state electrolyte hinders their practical application. In this work, the solid-liquid hybrid electrolyte S-Li1.3Al0.3Ti1.7(PO4)3-LE05(S-LATP-LE05) (LATP: Li1.5Al0.5Ti1.5 (PO4)3) sheet is prepared by dropping liquid electrolyte (LE) with appropriate FeF2 into spark plasma sintering S-LATP (solid-liquid hybrid electrolyte), which shows high-density and high-ionic-conductivity (5.78×10−4 S/cm). When the amount of FeF2 is 0.5 wt% , the interfacial properties between the anode and electrolyte are improved, and the S-LATP is well protected by LiF-rich (solid electrolyte interface) (SEI) interface in cycling process. The Li|S-LATP-LE05|Li symmetric battery and full battery show better electrochemical performance and stability relatively. The overpotential of the Li|S-LATP-LE05|Li symmetric battery is smaller and shows more stable electrochemical performance after cycling for 350 h, revealing good compatibility with a lithium metal anode and can inhibit the growth of lithium dendrites effectively. The Li|S-LATP-LE05|LiFePO4 full battery delivers a specific discharge capacity of 160 mA·h/g at 0.2C for 50 cycles. The corresponding coulombic efficiency is about 99.9% and displays better rate performance compared with the battery without FeF2 LE.

Appropriate FeF2 enhancing interface stability of lithium battery with solid-liquid hybrid electrolyte
Graphical Abstract
Original ResearchVol. 32, Issue 10 • pp. 3748-3766DOI: 10.1007/s11771-025-6098-9Jan 15, 2025

A novel and clean process for selective recovery of lithium from spent LiFePO4 cathode material by oxidative roasting-water leaching process

Authors: BI Xiao-long, MU Wen-ning, ZHANG Shi-xun, LI Meng, LEI Xue-fei, LUO Shao-hua

The recovery of lithium from spent lithium-ion batteries (LIBs) is of great importance in addressing lithium shortages and environmental issues. In this study, a novel and clean process for selective separation of lithium from spent LiFePO4 cathode material by low temperature oxidative roasting and water leaching was proposed. The effect of several important factors, such as roasting temperature, roasting time, and molar ratio of ferric chloride (FeCl3∙6H2O) to lithium iron phosphate (LFP), on the leaching efficiency of lithium and iron was systematically investigated by using single factor experimental method. The results show that approximately 97.1% lithium element was recovered by being converted to water-soluble LiCl at a roasting temperature 350 ℃, a roasting time 120 min and a FeCl3∙6H2O/LFP molar ratio of 1:1, and iron element was enriched in the leaching residue in the form of insoluble FePO4. High-purity lithium carbonate products could be prepared from the leching solution by adding Na2CO3 after removing iron. The establishment of new cleaning process can provide a scalable, environmentally friendly and simple way to recover valuable metals from spent LFP batteries.

A novel and clean process for selective recovery of lithium from spent LiFePO4 cathode material by oxidative roasting-water leaching process
Graphical Abstract
Original ResearchVol. 32, Issue 10 • pp. 3693-3707DOI: 10.1007/s11771-025-6095-zJan 15, 2025

Effect of rolling passes on AZ31 Mg alloy subjected to cross-rolling and cryogenic treatment

Authors: LU Li-wei, PANG Hao-ran, SHEN Tian-yuan, XI Yu-ze, WU Yu-juan, WANG Wen, JING Lei, LIU Gang

In this paper, the multi cross-rolling and cryogenic treatment were adopted to process the AZ31 Mg alloy to study the influence of passes and cryogenic treatment on cross-rolled AZ31 Mg alloy. The tensile properties and hardness were tested. The microstructure was characterized using electron backscatter diffraction (EBSD), transmission electron microscopy (TEM), and scanning electron microscopy (SEM) in order to elucidate the influencing mechanism. The results indicate that the treatment method can significantly improve the mechanical properties of AZ31 Mg alloy. The 3-pass sample processed by cryogenic treatment shows the highest strength (351 MPa) and has the highest hardness (76.1HV) and best hardness uniformity (standard deviation=0.9HV). The 2-pass sample has the highest ductility among all the samples but poor hardness evenness. The strengthening mechanism of 3-pass sample can be attributed to the fine grains, bimodal structure, high dislocation density, and precipitation strengthening. Due to repeated heat preservation of 4-pass and 5-pass, their comprehensive performances decrease.

Effect of rolling passes on AZ31 Mg alloy subjected to cross-rolling and cryogenic treatment
Graphical Abstract
Original ResearchVol. 32, Issue 9 • pp. 3493-3513DOI: 10.1007/s11771-025-6060-xJan 15, 2025

Innovative pillar recovery method integrating gob-side entry driving and directional roof-cutting for thick-hard roof coal seams

Authors: WU Yi-yi, YE Qiu-cheng, GAO Yu-bing, ZHANG Xing-xing, HE Man-chao

To enhance the recuperation rate of the mine and comply with the stipulations of green mining technology, it is vital to expeditiously recuperate the coal pillar resources in the final stage, thus preventing the considerable squandering of resources. The coal pillar resource of the main roadway and its branch roadway constitutes a significant recovery subject. Its coal pillar shape is regular and possesses a considerable strike distance, facilitating the arrangement of the coal pillar recovery working face (CPRWF) for mining operations. However, for the remaining coal pillars with a thick and hard roof (THF) and multiple tectonic zones, CPRWF encounters challenges in selecting an appropriate layout, managing excessive roof pressure, and predicting mining stress. Aiming at the roadway coal pillar group with THF and multi-structural areas in specific projects, a method of constructing multi-stage CPRWF by one side gob-side entry driving (GSED) and one side roadway reusing is proposed. Through theoretical calculation of roof fracture and numerical simulation verification, combined with field engineering experience and economic analysis, the width of the narrow coal pillar (NCP) in the GSED is determined to be 10 m and the length of the CPRWF is 65 m. Concurrently, the potential safety hazard that the roof will fall asymmetrically and THF is difficult to break during CPRWF mining after GSED is analyzed and verified. Then, a control method involving the pre-cutting of the roof in the reused roadway before mining is proposed. This method has been shown to facilitate the complete collapse of THF, reduce the degree of mine pressure, and facilitate the symmetrical breaking of the roof. Accordingly, a roof-cutting scheme based on a directional drilling rig, bidirectional shaped polyvinyl chloride (PVC) pipe, and emulsion explosive was devised, and the pre-splitting of 8.2 m THF was accomplished. Field observations indicate that directional cracks are evident in the roof, the coal wall is flat during CPRWF mining, and the overall level of mining pressure is within the control range. Therefore, the combined application of GSED and roof-cutting technology for coal pillar recovery has been successfully implemented, thereby providing new insights and engineering references for the construction and pressure relief mining of CPRWF.

Innovative pillar recovery method integrating gob-side entry driving and directional roof-cutting for thick-hard roof coal seams
Graphical Abstract
Original ResearchVol. 32, Issue 9 • pp. 3514-3538DOI: 10.1007/s11771-025-6074-4Jan 15, 2025

An innovative N00 mining approach for protecting entries and mining panels

Authors: ZHANG Jun, HE Man-chao, WANG Ya-jun, YANG Gang, HOU Shi-lin, CHEN Yu-wen, KANG Xu-hui, SHI Zhen, FU Qiang, DU Fu-kang

Addressing the issues of significant entry settlement and severe mining pressure manifestations in the conventional 121 approach, an innovative N00 approach is proposed. By comparing the mining process and entry formation process of different approaches, the characteristics of entry roof settlement evolution under different approaches are obtained. The N00 approach, which incorporates roof cutting and NPR cable support, optimizes the mining and entry formation process to reduce the settlement phase of entry roof, decreases the settlement of entry roof, and enhances the steadiness of entry roof. The N00 approach modifies the entry roof structure through roof cutting and establishes a hydraulic support load mechanics model for the mining panel to derive the theoretical load pressure formula for the N00 approach’s hydraulic support. Compared with the conventional 121 approach, the pressure on the N00 approach’s hydraulic support is reduced. Empirical data obtained through field monitoring demonstrate that the N00 approach has reduced the roof settlement of the entry and weakened the mining pressure manifestation at the mining panel, achieving the goal of protecting the entry and mining panel.

An innovative N00 mining approach for protecting entries and mining panels
Graphical Abstract
Original ResearchVol. 32, Issue 8 • pp. 3111-3123DOI: 10.1007/s11771-025-6054-8Jan 15, 2025

Quantifying influence of single particle shape and loading rate on mechanical properties of steel slag

Authors: Yang Hao, Wen Hui-shan, Zhang Jun-hui, Liu Ke, Xing Yi, Wu Meng-meng

As a typical solid waste from the iron and steel, the mechanical properties of steel slag are regarded as the core basis for realizing its resource recycling. To explore the influence of shape and external loading speed on the crushing characteristics of steel slag, single particle crushing tests were carried out. The research focuses on the correlation between parameters such as the load−displacement relationship of single particles, crushing mode, crushing energy, and Weibull modulus, as well as external loading rate and quantified morphological parameters. The results show that the single particle crushing modes of steel slag mainly consist of three modes: through-splitting, complete fragmentation and local cutting; Compared with natural aggregates or recycled materials, steel slag particles are found to potentially exhibit higher compressive strength and the increase in loading rate further accelerates the occurrence of particle crushing behavior; Significant impacts on the crushing mode and characteristic stress of steel slag particles are exerted by their shape differences, and the energy release mode is jointly regulated by shape and loading rate. This research provides theoretical guidance and technical support for the diversified utilization of steel slag single particles, a new type of solid waste resource.

Quantifying influence of single particle shape and loading rate on mechanical properties of steel slag
Graphical Abstract
Original ResearchVol. 32, Issue 5 • pp. 1955-1972DOI: 10.1007/s11771-025-5900-zJan 15, 2025

A novel asymptotic linear method for micro-pressure wave mitigation at high-speed maglev tunnel exit: A case study with various open ratios on tunnel hoods

Authors: ZHANG Jie, ZHANG Mo-lin, HAN Shuai, LIU Tang-hong, GAO Guang-jun

A high-speed train travelling from the open air into a narrow tunnel will cause the “sonic boom” at tunnel exit. When the maglev train’s speed reaches 600 km/h, the train-tunnel aerodynamic effect is intensified, so a new mitigation method is urgently expected to be explored. This study proposed a novel asymptotic linear method (ALM) for micro-pressure wave (MPW) mitigation to achieve a constant gradient of initial compression waves (ICWs), via a study with various open ratios on hoods. The properties of ICWs and MPWs under various open ratios of hoods were analyzed. The results show that as the open ratio increases, the MPW amplitude at the tunnel exit initially decreases before rising. At the open ratio of 2.28%, the slope of the ICW curve is linearly coincident with a supposed straight line in the ALM, which further reduces the MPW amplitude by 26.9% at 20 m and 20.0% at 50 m from the exit, as compared to the unvented hood. Therefore, the proposed method effectively mitigates MPW and quickly determines the upper limit of alleviation for the MPW amplitude at a fixed train-tunnel operation condition. All achievements provide a new potential measure for the adaptive design of tunnel hoods.

A novel asymptotic linear method for micro-pressure wave mitigation at high-speed maglev tunnel exit: A case study with various open ratios on tunnel hoods
Graphical Abstract
Original ResearchVol. 32, Issue 8 • pp. 2783-2794DOI: 10.1007/s11771-025-6041-0Jan 15, 2025

Influence of pre-compression and pre-aging on precipitation behavior in casting Mg-9.8Sn-3.0Zn alloy

Authors: LIU Yun, LIU Chao-qiang, NI Song, SONG Min

The effects of pre-compression and pre-aging on the age-hardening response and microstructure of Mg-9.8Sn-3.0Zn (wt.%) alloy have been investigated via hardness test and advanced electron microscopy. The alloy subjected to both pre-compression and pre-aging exhibits the most refined and densest distribution of precipitates upon aging at 200 ℃, leading to the superior age-hardening performance observed in the alloy. Comparatively, the alloy that underwent only pre-aging displayed a greater number density of precipitates than its counterpart that was neither pre-compressed nor pre-aged when both were aged to their peak conditions at 200 ℃, indicating an enhanced age-hardening response in the pre-aged alloy. The precipitates in these three peak-aged alloys consist of Mg2Sn and MgZn2 phases. The reason why the pre-aged alloy has a higher number density of precipitates than the directly aged alloy is that MgZn2 phase formed during pre-aging can serve as heterogeneous nucleation site for the formation of Mg2Sn. The reason why the pre-compression and pre-aged alloy has the highest number density of precipitates is that Mg3Sn and MgZn2 phases formed during pre-aging, alongside lattice defects introduced during pre-compression, collectively act as effective heterogeneous nucleation sites for the formation of Mg2Sn during the subsequent aging at 200 ℃.

Influence of pre-compression and pre-aging on precipitation behavior in casting Mg-9.8Sn-3.0Zn alloy
Graphical Abstract