SinoTechIntel Academic Portal
🏛️ Key Research Academy16 Indexed Works

Huazhong University of Science and Technology

Verified scientific contributions, CAS laboratory outputs, clinical trial papers, and engineering breakthroughs produced by researchers and faculty affiliated with Huazhong University of Science and Technology.

International Journal of Mining Science and Technology2026

Towards sustainable lunar habitats with ISRU in Chang’E mission: Mechanical–energy evolution and damage mechanisms of LPBF-printed lunar regolith simulate

Authors: Sheng Li, Xinyi Li, Yuyue Gao, Bo Zhou, Yan Zhou, Jian Song, Cheng Zhou, Wei Yao, Lieyun Ding

Targeting Chang’E-8 mission’ in-situ resource utilization (ISRU) for sustainable lunar habitats, laser powder bed fusion (LPBF) provides a viable pathway for in-situ additive manufacturing of lunar regolith. To elucidate mission relevant mechanical behavior and failure mechanisms of LPBF fabricated lunar regolith simulants, mare type and highland type simulant specimens were produced. Microstructural characterization, mechanical test coupled with three-dimensional digital image correlation (3D-DIC), and an energy-dissipation framework were employed for comprehensive analysis. The pristine highland specimens achieved 5.79 MPa and a peak strain of 0.13 (50 mm × 50 mm × 30 mm), significantly outperforming their mare counterparts. Wire-cutting to 20 mm × 20 mm × 20 mm lowered strength by ∼ 20% and peak strain to 0.04, indicating cutting-induced defects reduce ductility. All specimens displayed multi-peaked stress–strain curves. 3D-DIC revealed band-type strain localization in pristine highland samples, diffuse strain patterns in cut highland samples, and highly tortuous, network-type bands in mare samples; the anisotropy index was also quantified. Fragmented particles exhibited fractal dimensions ranging from 1.6 to 2.0 (size 1.25–9 mm). Energy evolution progressed through three distinct stages: elastic energy storage, progressive energy dissipation delaying crack propagation, and final unstable collapse. An energy-based damage model was established and validated. The data and methods developed support Chang’E-8 missions’ ISRU demonstrations and establish a transferable framework toward sustainable lunar habitats.

Peer ReviewedView Paper
China Foundry2026

Intelligent design of cooling systems for aluminum alloy die-casting dies: A framework integrating topology optimization and particle swarm optimization

Authors: Le-chuan Li, Ya-jun Yin, Xu Shen, Wen Li, Xiao-yuan Ji, Chao-jian Liang, Wei Wei, Jian-xin Zhou

With the growing demand for lightweight and high-performance components in automotive and aerospace industries, aluminum alloy die-castings are evolving toward larger dimensions and thinner walls, posing significant challenges to thermal management during solidification. Traditional cooling channel designs often fail to ensure uniform temperature distribution, leading to defects such as shrinkage porosity and deformation. This study proposes an automated design framework integrating the moving morphable components (MMC) topology optimization method with particle swarm optimization (PSO) to generate efficient and manufacturable cooling channel layouts for A380 aluminum alloys. Firstly, a systematic initialization strategy was developed with component dimensions of 4-10 mm in width and 15-40 mm in length, along with discrete orientation angles. The optimization process effectively guided components toward high-temperature regions identified through numerical simulation, followed by post-processing operations including temperature-based sorting, overlap removal, and component interconnection. The final design with 20 retained components was selected. Then, castings with a conventional cooling system and without any cooling system were employed as benchmark cases for comparison with the current optimized design. Compared with the conventional and no-cooling cases, the current cooling system exhibits a consistently lower temperature standard deviation after 30 s, maintains superior thermal uniformity throughout solidification, and achieves this improvement without comprising the average temperature.

Peer ReviewedView Paper
China Foundry2026

Factors influencing high-temperature compressive strength of alkaline phenolic resin-bonded sand

Authors: Xin Peng, Yu-yang Qi, Peng Yu, Peng Wan, Zhen-wei Liu, Wen Li, Xu Shen, Xiao-yuan Ji, Ya-jun Yin, Yuan-cai Li, Jian-xin Zhou

During the casting process, no-bake resin-bonded sand molds and cores rapidly heat up upon contact with high-temperature molten metal, causing dramatic changes in the resin binder system and a significant deterioration in mechanical properties, which subsequently leads to casting defects. To reveal the mechanism behind the evolution of high-temperature performance, the effects of resin content, base sand type, and particle size on the compressive strength of alkaline phenolic no-bake resin-bonded sand at temperatures ranging from 600 °C to 1,000 °C were investigated. The results show that the temperature range of 600-800 °C represents the primary stage of strength loss, corresponding to intense resin decomposition. Meanwhile, structural reorganization of the carbon skeleton above 900 °C can lead to a partial recovery of strength. This study provides key data and theoretical support for understanding the high-temperature mechanical behavior of resin-bonded sand and its relationship with casting defects.

Peer ReviewedView Paper
China Foundry (中国铸造 - 英文版)2026

Automatic gating and riser system design and defect control for K4169 superalloy guide blade casting based on parametric 3D modeling-simulation integrated system

Authors: Le-chuan Li, Ya-jun Yin, Bing-zheng Fan, Guo-yan Shui, Xiao-yuan Ji, Jian-xin Zhou, Lei Jin

Automation and intelligence have become the primary trends in the design of investment casting processes. However, the design of gating and riser systems still lacks precise quantitative evaluation criteria. Numerical simulation plays a significant role in quantitatively evaluating current processes and making targeted improvements, but its limitations lie in the inability to dynamically reflect the formation outcomes of castings under varying process conditions, making real-time adjustments to gating and riser designs challenging. In this study, an automated design model for gating and riser systems based on integrated parametric 3D modeling-simulation framework is proposed, which enhances the flexibility and usability of evaluating the casting process by simulation. Firstly, geometric feature extraction technology is employed to obtain the geometric information of the target casting. Based on this information, an automated design framework for gating and riser systems is established, incorporating multiple structural parameters for real-time process control. Subsequently, the simulation results for various structural parameters are analyzed, and the influence of these parameters on casting formation is thoroughly investigated. Finally, the optimal design scheme is generated and validated through experimental verification. Simulation analysis and experimental results show that using a larger gate neck (24 mm in side length) and external risers promotes a more uniform temperature distribution and a more stable flow state, effectively eliminating shrinkage cavities and enhancing process yield by 15%.

Peer ReviewedView Paper
Transactions of Nonferrous Metals Society of China (中国有色金属学报)2025

Multiscale investigation of oxidation mechanism in AlCrSiN multilayer coatings via experiments and ab initio molecular dynamics

Authors: Ji-yuan LIU, Shu-bing HU, Bo PENG, Jing-jing TIAN, Si-qi ZENG, Hai-xin CHANG, Hong-ya LI, Jin-ke YU, Fei GUO

An advanced AlCrSiN/AlCrN/CrN/Cr multilayer coating was developed via hybrid multiarc ion plating and high-power impulse magnetron sputtering. The multilayer design enhanced the substrate–coating compatibility, achieving a critical load of 87.8 N. Silicon doping induced nanocrystallization and amorphization, increasing the hardness to 26 GPa. At high temperatures, a nanoscale Cr-rich (Cr,Al)2O3 layer was formed, effectively inhibiting oxygen diffusion. The coating underwent unique phase transformations, during which Cr2N and amorphous Si3N4 were converted into dispersed SiCr3 nanoparticles, which stabilized Cr atoms and suppressed their outward diffusion. Ab initio molecular dynamics simulations revealed that Cr atoms exhibited higher chemical activity and oxygen-capture capability than Al atoms and Si atoms served as diffusion barriers by pinning onto the oxidized surface, considerably improving the oxidation resistance of the coating.

Peer ReviewedView Paper
Journal of Semiconductors (半导体学报 - 中国科学院半导体研究所)2025

A high reliability NOR flash cell in 50 nm node technology

Authors: Kevin Fang, Wei Wang, Yibai Xue, Fan Wang, Dong Pan, Yi Li, Jerry Zhou

Along with NOR flash cell scaling down, dielectric burnout has gradually become one of the most important factors which affects product reliability, especially for high dropout voltage films. In this study, we demonstrate a reliability-enhanced NOR flash cell in 50 nm node technology through structural optimization of floating gate (FG) dimensions and active area profile. By synergistically increasing FG thickness, reducing FG width, and tuning cell-open depth, the control gate-to-active area corner distance expands by 22%, suppressing peak electric fields by 29% vertically and 18% horizontally. This structural innovation achieves: (1) 100× reduction in early-cycle burnout failures, (2) 7.38× time dependent dielectric breakdown lifetime improvement, while maintaining data retention and accelerating programming/erasing speeds by 15.4%/7.3%. The enhanced reliability enables 97.5% reduction in Fowler−Nordheim stress time during characterization program testing, providing a cost-effective solution for automotive-grade flash memories.

Peer ReviewedView Paper
Journal of Semiconductors (半导体学报 - 中国科学院半导体研究所)2025

Optimization and defect control in photoresist etch back processes for advanced semiconductor technologies

Authors: Ting Lei, Zhehong Liu, Zhiwen Liu, Guangjie Xue, Chun Sun, Jun Zhou, Xiangshui Miao

The introduction of high-k/metal gate (HK/MG) technology enables independent tuning of N-type metal−oxide−semiconductor (NMOS) and P-type metal−oxide−semiconductor (PMOS) threshold voltages, facilitating advanced nodes and improving overall chip performance. However, severe pattern loading effects during PMOS device fabrication pose challenges in dummy poly removal. This work reports the optimization of the photoresist etch back (PREB) process, providing a wider process window for subsequent AL CMP. By tuning the PR coating uniformity to 1.6% and applying four-zone electrostatic chuck (ESC) temperature control, the wafer-level uniformities of PR, SiN, and SiO2 were reduced to 6.3%, 2.3%, and 5.1%, respectively. An optimized over etch (OE) recipe with a high selectivity of PR : SiN : SiO2 ≈ 1 : 1 : 6 effectively balanced gate height loading between N- and PMOS regions. Furthermore, precise EB1 time tuning enabled defect removal, while advanced KLA inspection ensured early detection of critical failure modes. Collectively, these measures establish a robust and stable PREB process for advanced logic device fabrication.

Peer ReviewedView Paper
China Foundry2025

A new oolitic content test method for green sand by repeated approximation

Authors: Yu-yang Qi, Jian-xin Zhou, Xin Peng, Si-yuan Pan, Ya-jun Yin, Xiao-yuan Ji, Yuan-cai Li, Peng-fei Lin, Peng Wan

The reuse of green sand in casting production is hindered by the accumulation of oolitic deposits, primarily composed of clay binder with surface degradation, which may adversely affect the the moulding sand performance. Currently, there is a lack of standardized methods for quantifying the oolitic content. Accurate measurement of oolitic content is of great significance to the reuse of green sand. Attempts to determine oolitic content using potassium hydroxide (KOH) and phosphoric acid (H3PO4) methods encounter challenges due to their excessive reactions with SiO2 in the sand. In this study, an improved method for measuring the oolitic content of green sand with repeated approximations was proposed. This method judges the chemical activity of the sample surface through the change of its mass to accurately obtain the mass of the reaction oolitic deposits. The test result of the used sand samples from the foundry shows that the oolitic deposits are completely removed after reacting with KOH solution three times at 300 °C for 20 min. SEM and EDS also show that after three times of reactions, the surface of green sand becomes smooth and the content of Al-containing oolitic deposits is very low. This indicates that the method can accurately control the extent of the reaction. Implementation of this method at Huangshi Dongbei Casting Co., Ltd. has yielded consistent and reliable test results, effectively mirroring variations in green sand oolitic content on the production line. This new method is expected to be widely adopted to improve the efficiency and quality of reused green sand in casting operations.

Peer ReviewedView Paper
China Foundry2025

Preparation of soluble ceramic cores via additive manufacturing technology: A review

Authors: Xiao-peng Yu, Wen-ming Jiang, Yun-xia Wang, Li Yang, Zi-wei Peng, Zi-tian Fan

Ceramic cores are key components in the production of castings with complex cavity structures. With the continuous development of the aerospace field, the demand for the castings with complex cavity structures is increasing. When using insoluble ceramic cores for casting, there is a significant challenge in removing complex blind cavities, which severely affects the completeness of the shape of the castings. Soluble ceramic cores can disintegrate when placed in water, greatly simplifying the removal process of cores and ensuring the complete formation of castings with complex cavity structures. Additive manufacturing technology, compared to traditional methods for preparing the soluble ceramic cores, does not require molds and can achieve direct forming of complex cores, simplifying the preparation process and reducing production time and costs. Nowadays, various additive manufacturing technologies, such as stereolithography (SL), selective laser sintering (SLS), direct ink writing (DIW), and binder jetting (BJ) technologies, have been successfully applied to the preparation of the ceramic cores. This paper analyzed the advantages and limitations of various additive manufacturing technologies, reviewed the research progress and raw material classifications of soluble ceramic cores prepared by these technologies, and looked forward to the future developments in the preparation of soluble ceramic cores using additive manufacturing technologies.

Peer ReviewedView Paper
China Foundry2025

Contextual design and real-time verification for agile casting design

Authors: Dong Xiang, Chu-hao Zhou, Xuan-pu Dong, Shu-ren Guo, Yan-song Ding, Hua-tang Cao

In the foundry industries, process design has traditionally relied on manuals and complex theoretical calculations. With the advent of 3D design in casting, computer-aided design (CAD) has been applied to integrate the features of casting process, thereby expanding the scope of design options. These technologies use parametric model design techniques for rapid component creation and use databases to access standard process parameters and design specifications. However, 3D models are currently still created through inputting or calling parameters, which requires numerous verifications through calculations to ensure the design rationality. This process may be significantly slowed down due to repetitive modifications and extended design time. As a result, there are increasingly urgent demands for a real-time verification mechanism to address this issue. Therefore, this study proposed a novel closed-loop model and software development method that integrated contextual design with real-time verification, dynamically verifying relevant rules for designing 3D casting components. Additionally, the study analyzed three typical closed-loop scenarios of agile design in an independent developed intelligent casting process system. It is believed that foundry industries can potentially benefit from favorably reduced design cycles to yield an enhanced competitive product market.

Peer ReviewedView Paper
China Foundry2025

Influence of surface layer slurry temperature on surface cracks and holes of ZTC4 titanium alloy by investment casting

Authors: Wei-dong Li, Xu-na Shi

In this work, the influences of surface layer slurry at different temperatures (10 °C, 14 °C, 18 °C, 22 °C) on wax patterns deformation, shrinkage, slurry coating characteristics, and the surface quality of the casting were investigated by using a single factor variable method. The surface morphologies of the shell molds produced by different temperatures of the surface (first) layer slurries were observed via electron microscopy. Furthermore, the microscopic composition of these shell molds was obtained by EDS, and the osmotic effect of the slurry on the wax patterns at different temperatures was also assessed by the PZ-200 Contact Angle detector. The forming reasons for the surface cracks and holes of thick and large ZTC4 titanium alloy by investment casting were analyzed. The experimental results show that the surface of the shell molds prepared by the surface layer slurry with a low temperature exhibits noticeable damage, which is mainly due to the poor coating performance and the serious expansion and contraction of wax pattern at low temperatures. The second layer shell material (SiO2, Al2O3) immerses into the crack area of the surface layer, contacts and reacts with the molten titanium to form surface cracks and holes in the castings. With the increase of the temperature of surface layer slurry, the damage to the shell surface tends to weaken, and the composition of the shell molds’ surface becomes more uniform with less impurities. The results show that the surface layer slurry at 22 °C is evenly coated on the surface of the wax patterns with appropriate thickness, and there is no surface shell mold rupture caused by sliding slurry after sand leaching. The surface layer slurry temperature is consistent with the wax pattern temperature and the workshop temperature, so there is no damage of the surface layer shell caused by expansion and contraction. Therefore, the shell mold prepared by the surface layer slurry at this temperature has good integrity, isolating the contact between the low inert shell material and the titanium liquid effectively, and the ZTC4 titanium alloy cylinder casting prepared by this shell mold is smooth, without cracks and holes.

Peer ReviewedView Paper
Nano-Micro Letters2025

In Situ Polymerization in COF Boosts Li-Ion Conduction in Solid Polymer Electrolytes for Li Metal Batteries

Authors: Junchen Meng, Mengjia Yin, Kairui Guo, Xingping Zhou, Zhigang Xue

Solid polymer electrolytes (SPEs) have garnered considerable interest in the field of lithium metal batteries (LMBs) owing to their exceptional mechanical strength, excellent designability, and heightened safety characteristics. However, their inherently low ion transport efficiency poses a major challenge for their application in LMBs. To address this issue, covalent organic framework (COF) with their ordered ion transport channels, chemical stability, large specific surface area, and designable multifunctional sites has shown promising potential to enhance lithium-ion conduction. Here, we prepared an anionic COF, TpPa-COOLi, which can catalyze the ring-opening copolymerization of cyclic lactone monomers for the in situ fabrication of SPEs. The design leverages the high specific surface area of COF to facilitate the absorption of polymerization precursor and catalyze the polymerization within the pores, forming additional COF-polymer junctions that enhance ion transport pathways. The partial exfoliation of COF achieved through these junctions improved its dispersion within the polymer matrix, preserving ion transport channels and facilitating ion transport across COF grain boundaries. By controlling variables to alter the crystallinity of TpPa-COOLi and the presence of –COOLi substituents, TpPa-COOLi with partial long-range order and –COOLi substituents exhibited superior electrochemical performance. This research demonstrates the potential in constructing high-performance SPEs for LMBs.

Peer ReviewedView Paper
Nano-Micro Letters2025

Manipulating Interfacial Stability via Preferential Absorption for Highly Stable and Safe 4.6 V LiCoO2 Cathode

Authors: Long Chen, Xin He, Yiqing Chen, Youmin Hou, Yujie Zhang, Kangli Wang, Xinping Ai, Yuliang Cao, Zhongxue Chen

Elevating the upper cutoff voltage to 4.6 V could effectively increase the reversible capacity of LiCoO2 (LCO) cathode, whereas the irreversible structural transition, unstable electrode/electrolyte interface and potentially induced safety hazards severely hinder its industrial application. Building a robust cathode/electrolyte interface film by electrolyte engineering is one of the efficient approaches to boost the performance of high-voltage LCO (HV-LCO); however, the elusive interfacial chemistry poses substantial challenges to the rational design of highly compatible electrolytes. Herein, we propose a novel electrolyte design strategy and screen proper solvents based on two factors: highest occupied molecular orbital energy level and LCO absorption energy. Tris (2, 2, 2-trifluoroethyl) phosphate is determined as the optimal solvent, whose low defluorination energy barrier significantly promotes the construction of LiF-rich cathode/electrolyte interface layer on the surface of LCO, thereby eventually suppresses the phase transition and enhances Li+ diffusion kinetics. The rationally designed electrolyte endows graphite||HV-LCO pouch cells with long cycle life (85.3% capacity retention after 700 cycles), wide-temperature adaptability (−60–80 °C) and high safety (pass nail penetration). This work provides new insights into the electrolyte screening and rational design to constructing stable interface for high-energy lithium-ion batteries.

Peer ReviewedView Paper
Nano-Micro Letters2025

Functionalized Separators Boosting Electrochemical Performances for Lithium Batteries

Authors: Zixin Fan, Xiaoyu Chen, Jingjing Shi, Hui Nie, Xiaoming Zhang, Xingping Zhou, Xiaolin Xie, Zhigang Xue

The growing demands for energy storage systems, electric vehicles, and portable electronics have significantly pushed forward the need for safe and reliable lithium batteries. It is essential to design functional separators with improved mechanical and electrochemical characteristics. This review covers the improved mechanical and electrochemical performances as well as the advancements made in the design of separators utilizing a variety of techniques. In terms of electrolyte wettability and adhesion of the coating materials, we provide an overview of the current status of research on coated separators, in situ modified separators, and grafting modified separators, and elaborate additional performance parameters of interest. The characteristics of inorganics coated separators, organic framework coated separators and inorganic–organic coated separators from different fabrication methods are compared. Future directions regarding new modified materials, manufacturing process, quantitative analysis of adhesion and so on are proposed toward next-generation advanced lithium batteries.

Peer ReviewedView Paper
Chinese Journal of Mechanical Engineering2025

Mechanical Response and Superelastic Properties of Cu-11.85Al-3.2Mn-0.1Ti TPMS Structures Printed by Laser Powder Bed Fusion

Authors: Mingzhu Dang, Honghao Xiang, Jingjing Li, Chunsheng Ye, Chao Cai, Qingsong Wei

Triply periodic minimal surfaces (TPMS) are structures with smooth surfaces and excellent energy absorption properties. Combining new functional materials, such as shape memory alloys, with TPMS structures provides a novel and promising research field. In this study, three TPMS structures (Gyroid, Diamond, and Primitive) of Cu-11.85Al-3.2Mn-0.1Ti alloy were printed by laser powder bed fusion, which is favorable for the fabrication of complex structures. The manufacturing fidelity, mechanical response, and superelastic properties of the three structures were investigated. Stress distributions in the three structures during compression were analyzed by finite element (FE) simulation. The three structures were equipped with high-quality, glossy surfaces and uniform pores. However, due to powder adhesion and forming steps, there were volumetric errors and dimensional deviations between the samples and the CAD models. The errors were within 1.6% for the Gyroid and Diamond structures. The dimensional deviations at the nodes in the three structures were less than 0.09 mm. The microstructures of all structures were β1´ martensite, consistent with the cubic sample. Experimental results of compression showed that the structures underwent a layer-by-layer compression failure mode, and the Primitive structures exhibited a more pronounced oscillatory process. The Diamond structures showed the highest first fracture stress and strain of 164.67 MPa and 13.89%, respectively. It also possessed the lowest yield strength (61.97 MPa) and the best energy absorption properties (7.6 MJ/m3). Through the deformation analysis, the Gyroid and Diamond structures were found to fracture at a 45° direction, while the Primitive structures fractured horizontally. These findings were consistent with the results obtained from the FE simulation, which showed equivalent stress distributions. After applying various pre-strains, the Diamond structures displayed the highest superelastic strain of up to 3.53%. The superelastic recovery of all samples ranged from 63.5% to 71.5%.

Peer ReviewedView Paper
Nano-Micro Letters2025

Aggregation-Induced Emissive Scintillators: A New Frontier for Radiation Detection and Imaging

Authors: Xinyi Li, Jiafu Yu, Yinghao Fan, Yuting Gao, Guangda Niu

Aggregation-induced emission (AIE) is a unique phenomenon where certain organic materials exhibit enhanced luminescence in their aggregated states, overcoming the typical quenching observed in conventional organic materials. Since its discovery in 2001, AIE has driven significant advances in fields like OLEDs and biological imaging, earning recognition in fundamental research. However, its application in high-energy radiation detection remains underexplored. Organic scintillators, though widely used, face challenges such as low light yield and poor radiation attenuation. AIE materials offer promising solutions by improving light yield, response speed, and radiation attenuation. This review summarizes the design strategies behind AIE scintillators and their very recent applications in X-ray, γ-ray, and fast neutron detection. We highlight their advantages in enhancing detection sensitivity, reducing background noise, and achieving high-resolution imaging. By addressing the current challenges, we believe AIE materials will play a pivotal role in advancing future radiation detection and imaging technologies.

Peer ReviewedView Paper