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Rapid Outgassing of Hydrophilic TiO2 Electrodes Achieves Long-Term Stability of Anion Exchange Membrane Water Electrolyzers

Authors: Shajahan Shaik; Jeonghyeon Kim; Mrinal Kanti Kabiraz; Faraz Aziz; Joon Yong Park; Bhargavi Rani Anne; Mengfan Li; Hongwen Huang; Ki Min Nam; Daeseong Jo; Sang-Il Choi

DOI: 10.1007/s40820-025-01696-2Status: Verified Translated Edition
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Key Findings in This Report

• A super-hydrophilic electrode was developed by depositing porous NiFe nanoparticles onto annealed TiO2 nanotubes (NiFe/ATNT), facilitating rapid outgassing of nonpolar gases. • The NiFe/ATNT electrode exhibited an overpotential of 235 mV at 10 mA cm−2 for the oxygen evolution reaction in 1.0 M KOH and served as the anode in the AEMWE, achieving a current density of 1.67 A cm−2 at 1.80 V. • The AEMWE utilizing the NiFe/ATNT electrode demonstrated remarkable stability, maintaining operation for 1500 h at 0.50 A cm−2 under challenging thermal conditions of 80 ± 3 °C. • The study highlights the importance of electrode surface engineering for efficient gas bubble removal, which is critical for long-term performance of AEMWEs.