• Aging at 873 K for 2 h induces Al- and Ti-rich nano-oxide precipitates with an orthorhombic CMCM structure in selective laser melted CoCrFeMnNi/NiCoFeAlTi composites.
• The aged high-entropy alloy composite achieves an ultimate tensile strength of 731 MPa through multi-scale strengthening.
• Strengthening arises from combined precipitation strengthening, dislocation strengthening, and high lattice distortion caused by intragranular defects.
• Aging treatment effectively controls precipitate phases in complex multi-element alloys, offering a pathway for high-performance HEAC design.
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