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Official PDF TranslationInt. Journal of Minerals, Metallurgy and Materials (矿物冶金与材料学报)

Enhancing rheology and mechanical properties of DLP 3D-printed Si3N4 materials via composition optimization and gas-pressure sintering

Authors: Qing Qin; Gang Xiong; Lin Han; Yujuan Zhang; Zhen Shen; Changchun Ge

DOI: 10.1007/s12613-025-3106-xStatus: Verified Translated Edition
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Key Findings in This Report

• Optimized Si3N4 slurry formulation achieves 50 vol% solid content with low viscosity (2.48 Pa·s) and excellent stability, enabling high-precision DLP 3D printing. • Gas-pressure sintering dramatically enhances flexural strength from ~109 MPa to ~618 MPa, while maintaining high hardness (16.59 GPa) and improved fracture toughness (4.45 MPa·m1/2). • Crack deflection and bridging are identified as dominant toughening mechanisms, along with pull-out of rod-like β-Si3N4 grains, effectively mitigating crack propagation. • The study provides a pathway for fabricating complex Si3N4 ceramic components with superior mechanical properties via DLP, offering significant potential for advanced engineering applications.