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Effects of combined dynamic-static loading and acidic corrosion treatment on the mechanical properties and microstructure of shale

Authors: Kang Peng; Hankuo Zhang; Mao Jing; Yunge Zhao

DOI: 10.1016/j.ijmst.2025.12.012Status: Verified Translated Edition
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Key Findings in This Report

• Combined dynamic-static loading and acidic corrosion cause significantly more severe mechanical degradation in shale than either single damage mode, with a 20% HCl treatment reducing peak strength to 158.97 MPa. • The damage factor, characterized by longitudinal wave velocity, increases with acid concentration, indicating a direct correlation between acid exposure and shale structural damage. • Energy analysis reveals that combined damage reduces total and elastic strain energy while increasing dissipated energy, leading to more developed fractures and severe failure. • Microstructural analyses (XRD and SEM) show that acid erosion reduces carbonate content and, when combined with mechanical pre-damage, accelerates acid-rock reactions, increasing micro-interfacial pores and degrading structural integrity.