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Prof. Zhao CAO

Northeastern University, School of Resources and Civil Engineering, Shenyang, China

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Transactions of Nonferrous Metals Society of China (中国有色金属学报)2026DOI: 10.1016/S1003-6326(26)67066-5

Effects of oxidation roasting on surface characteristics and flotation behavior of bastnaesite

Oxidation roasting of bastnaesite was conducted to evaluate its impact on surface characteristics and flotation behavior. Experiments varied temperature, time, and O2 concentration. Increasing temperature promoted thermal decomposition, yielding Ce7O12, RE2O3, and REF3 as main phases. The Ce oxidation degree and REO grade of roasted products exceeded 85.00%. Roasting induced long, narrow, nearly parallel cracks within particles, increasing porosity and causing partial fragmentation. During flotation, dissolved rare earth ion concentration increased significantly, and surface hydrolysis formed rare earth hydroxyl compounds. Complete decomposition raised the required collector dosage to achieve recovery above 85.00%. This increase is attributed to enhanced particle wettability, altered collector adsorption, and deeper penetration into the porous structure. The findings provide a basis for optimizing flotation circuits treating roasted bastnaesite, particularly in iron-bearing rare earth deposits where pyrometallurgical pretreatment is employed.

Int. Journal of Mining Science and Technology (采矿与安全工程)2024DOI: 10.1016/j.ijmst.2024.12.006

Advancing the recovery of iron and rare earth elements from the solid waste at Bayan Obo

The storage of solid waste in Bayan Obo has resulted in significant resource wastage and environmental concerns. In this study, an efficient process was developed to recover iron and rare earth elements (REEs) from this waste by processes of hydrogen-based mineral phase transformation (HMPT), magnetic separation, and flotation. Under optimal HMPT conditions (525 °C, 12.5 min, and 30% H2 concentration), an iron concentrate with a TFe grade of 64.09% and a recovery of 95.33% was obtained. The magnetic properties of the solid waste were greatly enhanced by HMPT, allowing the effective magnetic separation of iron minerals. Further optimization of the flotation process resulted in a REEs concentrate with a rare earth oxide (REO) grade of 65%–70% and a REEs recovery of 60%–65%. Hematite was reduced to magnetite during HMPT, and bastnaesite was decomposed to REEs oxides and fluorides, and the particle structure was significantly destroyed. However, changes in monazite, fluorite, and barite were minimal.

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